Spectra

HNMR

MG_NMR.png

10/01/2021 18:17:46

False

Raman

MG_Raman.png

10/01/2021 18:07:31

False

ESI+ Mass Spectrum

MG_ESI_MS.png

10/01/2021 17:54:30

False

Infrared

MG_IR.png

10/01/2021 17:52:26

False

From Ngee Sing Chong FTIR Dye Library

Infrared

Allura Red FTIR.png

10/01/2021 17:48:54

False

HNMR

Allura Red NMR.png

10/01/2021 17:44:24

False

ESI- Mass Spectrum

Allura Red QTOFMS.png

10/01/2021 17:43:47

False

ESI- Mass Spectrum

Allura Red LC_MS.png

10/01/2021 17:30:53

False

9118756

HNMR

Boc-L-vinylglycine CAS 91028-39-6 HNMR.png

30/12/2020 08:46:50

False

HNMR from ChemWhat, Database of Chemicals & Manufacturers.

Raman

Allura Red AC_Raman_DKT.pdf

13/12/2020 17:12:02

False

Ngee Sing Chong's Raman Database Library

67824

HNMR

NMR-3 of Poly(ethylene glycol) diacrylate CAS 26570-48-9.png

09/12/2020 06:17:18

False

HNMR-3 from ChemWhat, Database of Chemicals & Manufacturers.

67824

HNMR

NMR-2 of Poly(ethylene glycol) diacrylate CAS 26570-48-9.png

09/12/2020 06:16:42

False

HNMR-2 from ChemWhat, Database of Chemicals & Manufacturers.

67824

HNMR

NMR-1 of Poly(ethylene glycol) diacrylate CAS 26570-48-9.png

09/12/2020 06:13:27

False

HNMR-1 from ChemWhat, Database of Chemicals & Manufacturers.

2D NMR 1H-13C Long-range correlation

HMBC SilylbetaCD.png

31/10/2020 23:08:59

False

2D 1H-13C gHMBCAD spectrum measured in CDCl3 at 298 K on a Bruker Avance III HD 600 MHz spectrometer equipped with a QCI 1H/13C/15N/31P proton-optimized quadrupole inverse cryoprobe with 1H and 13C cryochannels, using standard pulse sequences and processing routines available in Bruker TopSpin 3.6.2. 1D 1H and 13C NMR spectra are referenced to the CDCl3 residual signals (δ = 7.26 ppm and 77.16 ppm, respectively).

2D NMR 1H-13C Direct correlation

HSQC SilylbetaCD.png

31/10/2020 23:08:28

False

2D 1H-13C gHSQCAD spectrum measured in CDCl3 at 298 K on a a 600 MHz Varian DDR NMR spectrometer equipped with a 5 mm inverse-detection gradient (IDPFG) probehead, using standard pulse sequences and processing routines available in VnmrJ 3.2 C/Chempack 5.1. 1D 1H and 13C NMR spectra are referenced to the CDCl3 residual signals (δ = 7.26 ppm and 77.16 ppm, respectively).

2D NMR 1H-1H COSY

COSY SilylbetaCD.png

31/10/2020 23:08:00

False

2D 1H-1H gCOSY spectrum measured in CDCl3 at 298 K on a Bruker Avance III HD 600 MHz spectrometer equipped with a QCI 1H/13C/15N/31P proton-optimized quadrupole inverse cryoprobe with 1H and 13C cryochannels, using standard pulse sequences and processing routines available in Bruker TopSpin 3.6.2. 1D 1H NMR spectra are referenced to the CDCl3 residual signal (δ = 7.26 ppm).

CNMR

13C SilylbetaCD.dx

31/10/2020 23:07:26

False

13C NMR spectrum measured in CDCl3 at 298 K on a Bruker Avance III HD 600 MHz spectrometer equipped with a QCI 1H/13C/15N/31P proton-optimized quadrupole inverse cryoprobe with 1H and 13C cryochannels, using standard pulse sequences and processing routines available in Bruker TopSpin 3.6.2. Chemical shifts (δ) are referenced to the CDCl3 residual signal (δ = 77.16 ppm). 13C NMR (150 MHz, CDCl3, ppm) δ 102.1 (C-1), 81.9 (C-4), 73.8 (C-2), 73.5 (C-3), 72.7 (C-5), 61.8 (C-6), 26.1 (SiC(CH3)3), 18.4 (SiC(CH3)3), -4.9 (SiCH3), -5.0 (SiCH3).