| 10820 | HNMR | MG_NMR.png | 10/01/2021 18:17:46 | False | |
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| 10820 | Raman | MG_Raman.png | 10/01/2021 18:07:31 | False | |
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| 10820 | ESI+ Mass Spectrum | MG_ESI_MS.png | 10/01/2021 17:54:30 | False | |
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| 10820 | Infrared | MG_IR.png | 10/01/2021 17:52:26 | False | From Ngee Sing Chong FTIR Dye Library |
| 11588224 | Infrared | Allura Red FTIR.png | 10/01/2021 17:48:54 | False | |
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| 11588224 | HNMR | Allura Red NMR.png | 10/01/2021 17:44:24 | False | |
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| 11588224 | ESI- Mass Spectrum | Allura Red QTOFMS.png | 10/01/2021 17:43:47 | False | |
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| 11588224 | ESI- Mass Spectrum | Allura Red LC_MS.png | 10/01/2021 17:30:53 | False | |
| 9118756 | HNMR | Boc-L-vinylglycine CAS 91028-39-6 HNMR.png | 30/12/2020 08:46:50 | False | HNMR from ChemWhat, Database of Chemicals & Manufacturers. |
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| 11588224 | Raman | Allura Red AC_Raman_DKT.pdf | 13/12/2020 17:12:02 | False | Ngee Sing Chong's Raman Database Library
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| 67824 | HNMR | NMR-3 of Poly(ethylene glycol) diacrylate CAS 26570-48-9.png | 09/12/2020 06:17:18 | False | HNMR-3 from ChemWhat, Database of Chemicals & Manufacturers.
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| 67824 | HNMR | NMR-2 of Poly(ethylene glycol) diacrylate CAS 26570-48-9.png | 09/12/2020 06:16:42 | False | HNMR-2 from ChemWhat, Database of Chemicals & Manufacturers.
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| 67824 | HNMR | NMR-1 of Poly(ethylene glycol) diacrylate CAS 26570-48-9.png | 09/12/2020 06:13:27 | False | HNMR-1 from ChemWhat, Database of Chemicals & Manufacturers.
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| 9117549 | 2D NMR 1H-13C Long-range correlation | HMBC SilylbetaCD.png | 31/10/2020 23:08:59 | False | 2D 1H-13C gHMBCAD spectrum measured in CDCl3 at 298 K on a Bruker Avance III HD 600 MHz spectrometer equipped with a QCI 1H/13C/15N/31P proton-optimized quadrupole inverse cryoprobe with 1H and 13C cryochannels, using standard pulse sequences and processing routines available in Bruker TopSpin 3.6.2. 1D 1H and 13C NMR spectra are referenced to the CDCl3 residual signals (δ = 7.26 ppm and 77.16 ppm, respectively). |
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| 9117549 | 2D NMR 1H-13C Direct correlation | HSQC SilylbetaCD.png | 31/10/2020 23:08:28 | False | 2D 1H-13C gHSQCAD spectrum measured in CDCl3 at 298 K on a a 600 MHz Varian DDR NMR spectrometer equipped with a 5 mm inverse-detection gradient (IDPFG) probehead, using standard pulse sequences and processing routines available in VnmrJ 3.2 C/Chempack 5.1. 1D 1H and 13C NMR spectra are referenced to the CDCl3 residual signals (δ = 7.26 ppm and 77.16 ppm, respectively). |
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| 9117549 | 2D NMR 1H-1H COSY | COSY SilylbetaCD.png | 31/10/2020 23:08:00 | False | 2D 1H-1H gCOSY spectrum measured in CDCl3 at 298 K on a Bruker Avance III HD 600 MHz spectrometer equipped with a QCI 1H/13C/15N/31P proton-optimized quadrupole inverse cryoprobe with 1H and 13C cryochannels, using standard pulse sequences and processing routines available in Bruker TopSpin 3.6.2. 1D 1H NMR spectra are referenced to the CDCl3 residual signal (δ = 7.26 ppm). |
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| 9117549 | CNMR | 13C SilylbetaCD.dx | 31/10/2020 23:07:26 | False | 13C NMR spectrum measured in CDCl3 at 298 K on a Bruker Avance III HD 600 MHz spectrometer equipped with a QCI 1H/13C/15N/31P proton-optimized quadrupole inverse cryoprobe with 1H and 13C cryochannels, using standard pulse sequences and processing routines available in Bruker TopSpin 3.6.2. Chemical shifts (δ) are referenced to the CDCl3 residual signal (δ = 77.16 ppm). 13C NMR (150 MHz, CDCl3, ppm) δ 102.1 (C-1), 81.9 (C-4), 73.8 (C-2), 73.5 (C-3), 72.7 (C-5), 61.8 (C-6), 26.1 (SiC(CH3)3), 18.4 (SiC(CH3)3), -4.9 (SiCH3), -5.0 (SiCH3). |
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| 9117549 | HNMR | 1H SilylbetaCD.dx | 31/10/2020 23:06:47 | False | 1H NMR spectrum measured in CDCl3 at 298 K on a 600 MHz Varian DDR NMR spectrometer equipped with a 5 mm inverse-detection gradient (IDPFG) probehead, using standard pulse sequences and processing routines available in VnmrJ 3.2 C/Chempack 5.1. Chemical shifts (δ) are referenced to the CDCl3 residual signal (δ = 7.26 ppm). 1H NMR (600 MHz, CDCl3, ppm) δ 4.89 (d, J1,2 = 3.5 Hz, 7H, H-1), 4.04 (t, J = 9.2 Hz, 7H, H-3), 3.90 (dd, J6a,6b = 11.3 Hz, J5,6a = 2.9 Hz, 7H, H-6a), 3.71 (br d, J = 10.5 Hz, 7H, H-6b), 3.64 (dd, J2,3 = 9.6 Hz, J1,2 = 3.5 Hz, 7H, H-2), 3.62 (br s, 7H, H-5), 3.56 (t, J = 9.2 Hz, 7H, H-4), 0.87 (s, 63H, SiC(CH3)3), 0.04 (s, 21H, SiCH3), 0.03 (s, 21H, SiCH3). |
| 9161332 | 2D NMR 1H-13C Direct correlation | HSQC SilylgammaCD DMSO.png | 27/10/2020 22:20:34 | False | 2D 1H-13C gHSQCAD spectrum measured in DMSO-d6 at 298 K on a 1H NMR spectrum measured in DMSO-d6 at 298 K on a 600 MHz Varian DDR NMR spectrometer equipped with a 5 mm inverse-detection gradient (IDPFG) probehead, using standard pulse sequences and processing routines available in VnmrJ 3.2 C/Chempack 5.1. 1D 1H and 13C NMR spectra are referenced to the DMSO-d6 residual signals (δ = 2.50 ppm and 39.52 ppm, respectively). Please note that heptakis(6-O-tert-butyldimethylsilyl)-beta-cyclodextrin is poorly soluble in DMSO, and thus low concentration is reached within the tube, giving a very low signal-to-noise ratio in f1. |
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| 9161332 | 2D NMR 1H-1H COSY | COSY SilylgammaCD DMSO.png | 27/10/2020 22:20:04 | False | 2D 1H-1H gCOSY spectrum measured in DMSO-d6 at 298 K on a 1H NMR spectrum measured in DMSO-d6 at 298 K on a 600 MHz Varian DDR NMR spectrometer equipped with a 5 mm inverse-detection gradient (IDPFG) probehead, using standard pulse sequences and processing routines available in VnmrJ 3.2 C/Chempack 5.1. 1D 1H NMR spectra are referenced to the DMSO-d6 residual signal (δ = 2.50 ppm). |